By Faraday M., Crookes W.

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The c y c l i c pathway i s followed u n t i l a l l of the hydrogen atoms are exchanged by deuterium. The key to the mechanistic scheme i s formation and opening of the m e t a l l o c y c l e . ; ACS Symposium Series; American Chemical Society: Washington, DC, 1980. 2. ANDERSEN 43 4i- and 5i-Block Metals reaction of i t with deuterium to yield the perdeutoro-derivative strongly implies that the mechanistic scheme i s essentially correct. The observation that the hydrides, [(Me Si) N]3MH, extrude hydrogen and form the metallocycle is added support for the essential validity of the proposed mechanism.

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Kirmse, W. , 1971, Chapt. 3, S e c t i o n E. 53. W. Angew. Chem. I n t . , 1971, 10, 529-540. 54. , Topics C u r r . , 1976, 62, 173-251. 55. Reference 50, p. 72. 56. Reference 52, Chapt. 12. 57. , J. Am. Chem. , 1967, 89, 7112-7113. 58. , Coord. Chem. , 1977, 24, 1095. 59. , Advan. Chem. S e r . , 1976, 150, 266-272. 60. C. Chem. , 1975, 11, 393-397. 61. C. Advan. I n o r g . Chem. , 1972, 15, 259322. 62. W. submitted f o r publication. 63. J. unpublished results. 64. , I n o r g . , 1979, 18, 1165-1168, and references t h e r e i n .

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